Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K

doi:10.1007/s12204-013-1390-5

上海交通大学学报（英文版） ›› 2013, Vol. 18 ›› Issue (2): 253-256.doi: 10.1007/s12204-013-1390-5

• 论文 • 上一篇

Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K

FAN Yue-lei (范月蕾), PENG Hua-song* (彭华松), XIE Kan (谢侃), ZHANG Xue-hong (张雪洪)

(School of Life Science and Biotechnology; State Key Laboratory of Microbial Metabolism, Shanghai Jiaotong University, Shanghai 200240, China)

出版日期:2013-04-30 发布日期:2013-05-10
通讯作者: PENG Hua-song (彭华松) E-mail: hspeng@sjtu.edu.cn

Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K

FAN Yue-lei (范月蕾), PENG Hua-song* (彭华松), XIE Kan (谢侃), ZHANG Xue-hong (张雪洪)

(School of Life Science and Biotechnology; State Key Laboratory of Microbial Metabolism, Shanghai Jiaotong University, Shanghai 200240, China)

Online:2013-04-30 Published:2013-05-10
Contact: PENG Hua-song (彭华松) E-mail: hspeng@sjtu.edu.cn

摘要/Abstract

摘要： Compound of 1-hydroxyphenazine (1-OH-PHZ) is an important fungicide in agricultural production. The ranges of 1-OH-PHZ solubilities in dichloromethane at temperature of 278.5—308.5 K and in ethyl acetate, methanol and water at temperature of 278.5—333.5 K were measured using the analytical stirred flask method at barometric pressure. The color of the liquid remained unchanged throughout. The solubilities of 1-OH-PHZ in water, methanol, ethyl acetate and dichloromethane increased orderly and these solubilities also increased with increasing the temperature. The experimental data was correlated by the modified Apelblat equation. The root mean square deviations were all within 0.5% and the maximum relative average deviation was 5.2%. The calculated solubility shows a good relationship with the experimental solubility.

关键词: solubility, 1-hydroxyphenazine (1-OH-PHZ), fungicide, correlation

Abstract: Compound of 1-hydroxyphenazine (1-OH-PHZ) is an important fungicide in agricultural production. The ranges of 1-OH-PHZ solubilities in dichloromethane at temperature of 278.5—308.5 K and in ethyl acetate, methanol and water at temperature of 278.5—333.5 K were measured using the analytical stirred flask method at barometric pressure. The color of the liquid remained unchanged throughout. The solubilities of 1-OH-PHZ in water, methanol, ethyl acetate and dichloromethane increased orderly and these solubilities also increased with increasing the temperature. The experimental data was correlated by the modified Apelblat equation. The root mean square deviations were all within 0.5% and the maximum relative average deviation was 5.2%. The calculated solubility shows a good relationship with the experimental solubility.

Key words: solubility, 1-hydroxyphenazine (1-OH-PHZ), fungicide, correlation

中图分类号:

TQ 013

FAN Yue-lei (范月蕾), PENG Hua-song* (彭华松), XIE Kan (谢侃), ZHANG Xue-hong (张雪洪). Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K[J]. 上海交通大学学报（英文版）, 2013, 18(2): 253-256.

FAN Yue-lei (范月蕾), PENG Hua-song* (彭华松), XIE Kan (谢侃), ZHANG Xue-hong (张雪洪). Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K[J]. Journal of shanghai Jiaotong University (Science), 2013, 18(2): 253-256.

参考文献

[1] Laursen J B, Nielsen J. Phenazine natural products: Biosynthesis, synthetic analogues, and biological activity [J]. Chemical Reviews, 2004, 104(3): 1663-1685.
[2] Badria F A, El-Naggar W A. Structures and antimicrobial activity of five phenazine pigments isolated from Pseudomonas aeruginosa [J]. Scientia Pharmaceutica, 1994, 62(4): 355-362.
[3] Kerr J R, Taylor G W, Rutman A, et al. Pseudomonas aeruginosa pyocyanin and 1-hydroxyphenazine inhibit fungal growth [J]. Journal of Clinical Pathology, 1999, 52(5): 385-387.
[4] Gibson J, Sood A, Hogan D A. Pseudomonas aeruginosa-candida albicans interactions: Localization and fungal toxicity of a phenazine derivative [J]. Applied and Environmental Microbiology, 2009, 75(2): 504-513.
[5] Issidorides C H, Atfah M A, Saboungi J J, et al. Application of 1, 2-diketones in the synthesis of phenazine oxides [J]. Tetrahedron, 1978, 34(2): 217-221.
[6] Barbero C, Miras M C, Kotz R, et al. Study of the structure and redox behaviour of poly(1-hydroxyphenazine) [J]. Synthetic Metals, 1999, 101(1-3): 23.
[7] Wang L H, Cheng Y Y. Solubility of puerarin in water, ethanol, and acetone from (288.2 to 328.2) K [J]. Journal of Chemical and Engineering Data, 2005, 50(4): 1375-1376.
[8] Li X N, Yin Q X, Chen W, et al. Solubility of hydroquinone in different solvents from 276.65 K to 345.10 K [J]. Journal of Chemical and Engineering Data, 2006, 51(1): 127-129.
[9] Lei Z Y, Hu Y H, Yang W G, et al. Solubility of 2-(2,4,6-trichlorophenoxy)-ethyl bromide in methanol, ethanol, propanol, isopropanol, acetonitrile, n-heptane, and acetone [J]. Journal of Chemical and Engineering Data, 2011, 56(5): 2714-2719.
[10] Wang W, Lu X H, Qin X J, et al. Solubility of pyoluteorin in water, dichloromethane, chloroform, and carbon tetrachloride from (278.2 to 333.2) K [J]. Journal of Chemical and Engineering Data, 2008, 53(9): 2241-2243.
[11] Kong X Q, Shea D, Gebreyes W A, et al. Novel hydrophobicity ruler approach for determining the octanol/water partition coefficients of very hydrophobic compounds via their polymer/solvent solution distribution coefficients [J]. Analytical Chemistry, 2005, 77(5): 1275-1281.
[12] Manzurola E, Apelblat A. Solubilities of Lglutamic acid, 3-nitrobenzoic acid, p-toluic acid, calcium-L-lactate, calcium gluconate, magnesium-DLaspartate, and magnesium-L-lactate in water [J]. Journal of Chemical Thermodynamics, 2002, 34(7): 1127-1136.

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Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K

Measurement and Correlation of the Solubility of 1-Hydroxyphenazine in Different Solvents at Temperature from 278.5 to 333.5K

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