Operation Analysis of PandaX-4T Ultra-High Purity Xenon Cryogenic Distillation System for Removal of Krypton

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  • 1. Institute of Refrigeration and Cryogenics, Shanghai Jiao Tong University, Shanghai 200240, China
    2. Institute of Nuclear and Particle Physics, Shanghai Jiao Tong University, Shanghai 200240, China
    3. Tsung-Dao Lee Institute, Shanghai Jiao Tong University, Shanghai 200240, China
    4. College of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China
    5. Paris Tech Elite Institute of Technology, Shanghai Jiao Tong University, Shanghai 200240, China

Received date: 2020-06-15

  Online published: 2021-06-08

Abstract

Based on the McCabe-Thiele (M-T) method and the conservation of mass and energy, the PandaX-4T collaboration group designs an efficient cryogenic distillation system to reduce the mole fraction of krypton in commercial xenon from 5×10-7 to 1×10-14. Since the ultra-high purity xenon cryogenic distillation system has completed the offline purification operation, it is necessary to conduct the corresponding operation analysis. Therefore, the stability and purification performance of the ultra-high purity xenon cryogenic distillation system are studied by analyzing the parameters such as temperature, pressure, flowrate, and mole faction of the product xenon in each operating stage. The PandaX-4T cryogenic distillation system has been operating stably for 1.5 m at a collection efficiency of 99% and a purification rate of 10 kg/h, and has purified 5.75 t of xenon. The experimental data show that the system is stable, safe, and reliable in all stages of operation, and the krypton concentration in product xenon is less than 7.99×10-12. The operation analysis of the PandaX-4T ultra-high purity xenon cryogenic distillation system has a theoretical research value and practical engineering significance, providing very important reference for optimization of distillation operation of the next stage.

Cite this article

YAN Rui, WANG Zhou, CUI Xiangyi, JU Yonglin, SHA Haidong, LI Shuaijie, HUANG Peiyao, WANG Xiuli . Operation Analysis of PandaX-4T Ultra-High Purity Xenon Cryogenic Distillation System for Removal of Krypton[J]. Journal of Shanghai Jiaotong University, 2021 , 55(7) : 834 -841 . DOI: 10.16183/j.cnki.jsjtu.2020.180

References

[1] APRILE E, DOKE T. Liquid xenon detectors for particle physics and astrophysics[J]. Reviews of Modern Physics, 2010, 82(3): 2053.
[2] AKIMOV D. Techniques and results for the direct detection of dark matter (review)[J]. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 2011, 628(1): 50-58.
[3] CHEPEL V, ARAÚJO H. Liquid noble gas detectors for low energy particle physics[J]. Journal of Instrumentation, 2013, 8(4): R04001.
[4] BERNABEI R, BELLI P, MONTECCHIA F, et al. New limits on particle dark matter search with a liquid xenon target-scintillator[J]. Physics Letters B, 1998, 436(3/4): 379-388.
[5] TAN A, XIAO M J, CUI X Y, et al. Dark matter results from first 98.7 days of data from the PandaX-II experiment[J]. Physical Review Letters, 2016, 117(12): 121303.
[6] CUI X Y, ABDUKERIM A, CHEN W, et al. Dark matter results from 54-ton-day exposure of PandaX-II experiment[J]. Physical Review Letters, 2017, 119(18): 181302.
[7] REN X X, ZHAO L, ABDUKERIM A, et al. Constraining dark matter models with a light mediator at the PandaX-II experiment[J]. Physical Review Letters, 2018, 121(2): 021304.
[8] ABE K, HOSAKA J, IIDA T, et al. Distillation of liquid xenon to remove krypton[J]. Astroparticle Physics, 2009, 31(4): 290-296.
[9] WANG Z, BAO L, HAO X H, et al. Design and construction of a cryogenic distillation device for removal of krypton for liquid xenon dark matter detectors[J]. The Review of Scientific Instruments, 2014, 85(1): 015116.
[10] WANG Z, BAO L, HAO X H, et al. Large scale xenon purification using cryogenic distillation for dark matter detectors[J]. Journal of Instrumentation, 2014, 9(11): P11024.
[11] APRILE E, AALBERS J, AGOSTINI F, et al. Removing krypton from xenon by cryogenic distillation to the ppq level[J]. European Physical Journal C, 2017, 77:1-12.
[12] FIEGUTH A, COLLABORATION X. Distillation column for the XENON1T experiment[J]. Journal of Physics: Conference Series, 2016, 718:042020.
[13] 崔祥仪. PandaX-II暗物质实验与PandaX-4T制冷循环与精馏系统[D]. 上海: 上海交通大学, 2019.
[13] CUI Xiangyi. PandaX-II dark matter experiment and the PandaX-4T cryogenics, circulation and distillation system[D]. Shanghai: Shanghai Jiao Tong University, 2019.
[14] 王舟, 张华, 巨永林. 暗物质探测器的液氙低温精馏系统研制[J]. 上海交通大学学报, 2013, 47(8): 1282-1286.
[14] WANG Zhou, ZHANG Hua, JU Yonglin. Design and construction of a cryogenic distillation system of liquid xenon for dark matter detector[J]. Journal of Shanghai Jiao Tong University, 2013, 47(8): 1282-1286.
[15] MCCABE W L, SMITH J C. Unit operations of chemical engineering[M]. 3rd ed. New York, NY, USA: McGraw-Hill, 1976.
[16] DOBI A, DAVIS C, HALL C, et al. Detection of krypton in xenon for dark matter applications[J]. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 2011, 665:1-6.
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