J Shanghai Jiaotong Univ Sci

Journal of Shanghai Jiaotong University(Science) >

2025 , Vol. 30 >Issue 2: 262 - 269

DOI: https://doi.org/10.1007/s12204-023-2597-8

Engieering and Technology

Piezoelectric Materials Full-Matrix Constants Characterization Based on Local Electrodes Using One Sample

Expand
  • National Key Laboratory of Science and Technology on Micro/Nano Fabrication; Department of Micro/Nano Electronics, Shanghai Jiao Tong University, Shanghai 200240, China

Accepted date: 2022-02-10

  Online published: 2025-03-21

Fold

Abstract

A novel characterization method for full-matrix constants of PZT-8 piezoceramics based on local electrodes excitation using one sample is proposed to avoid resonant peaks missing and overlapping in the inversion process of resonant ultrasound spectroscopy technology. Elastic matrix, which is sensitive to the resonance spectrum, is obtained by resonant ultrasound spectroscopy. Piezoelectric and dielectric matrices, which are sensitive to the capacitance of driving electrodes, are determined by capacitance inversion. The initial values of elastic constants are deviated by 30% to validate the reliability of this method. The relative errors between measured and inversed values of resonant frequencies are less than 1% and the relative errors of the capacitance are mostly less than 5%. The work has extensive applications in piezoelectric materials characterization.

Cite this article

Feng Qiyun, Wu Xiaosheng, Zhao Junjun, Zeng Zhaofeng, Li Jian, Yin Chengbin . Piezoelectric Materials Full-Matrix Constants Characterization Based on Local Electrodes Using One Sample[J]. Journal of Shanghai Jiaotong University(Science), 2025 , 30(2) : 262 -269 . DOI: 10.1007/s12204-023-2597-8

References

[1] JAFFE H. Piezoelectric ceramics [J]. Journal of the American Ceramic Society, 1958, 41(11): 494-498.
[2] CAO H, SCHMIDT V H, ZHANG R, et al. Elastic, piezoelectric, and dielectric properties of 0.58 Pb (Mg1/3Nb2/3)O3-0.42 PbTiO3 single crystal [J]. Journal of Applied Physics, 2004, 96(1): 549-554.
[3] SHANTHI M, LIM L C, RAJAN K K, et al. Complete sets of elastic, dielectric, and piezoelectric properties of flux-grown [011]-poled Pb (Mg1/3Nb2/3)O3- (28-32)% PbTiO3 single crystals [J]. Applied Physics Letters. 2008, 92(14): 189-191.
[4] YU TOPOLOV V, BOWEN C R. Inconsistencies of the complete sets of electromechanical constants of relaxor-ferroelectric single crystals [J]. Journal of Applied Physics, 2011, 109(9): 094107.
[5] LEISURE R G, WILLIS F A. Resonant ultrasound spectroscopy [J]. Journal of Physics: Condensed Matter, 1997, 9(28): 6001-6029.
[6] MIGLIORI A, MAYNARD J D. Implementation of a modern resonant ultrasound spectroscopy system for the measurement of the elastic moduli of small solid specimens [J]. Review of Scientific Instruments, 2005, 76(12): 121301.
[7] LI S, ZHENG L, JIANG W, et al. Characterization of full set material constants of piezoelectric materials based on ultrasonic method and inverse impedance spectroscopy using only one sample [J]. Journal of Applied Physics, 2013, 114(10): 104505.
[8] FRASER D B, LECRAW R C. Novel method of measuring elastic and anelastic properties of solids [J]. Review of Scientific Instruments, 1964, 35(9): 1113-1115.
[9] TANG L G, CAO W W. Temperature dependence of self-consistent full matrix material constants of lead zirconate titanate ceramics [J]. Applied Physics Letters, 2015, 106(5): 052902.
[10] XUAN S, LI S, DUN X, et al. A novel characterization method of piezoelectric composite material based on particle swarm optimization algorithm [J]. Applied Mathematical Modelling, 2019, 66: 322-331.
[11] TANG L G, TIAN H, ZHANG Y, et al. Temperature dependence of dielectric, elastic, and piezoelectric constants of [001]c poled Mn-doped 0.24Pb (In1/2Nb1/2)O3-0.46Pb(Mg1/3Nb2/3)O3-0.30PbTiO3 single crystal [J]. Applied Physics Letters, 2016, 108(8): 082901.
[12] TANG L G. Mode identification via temperature variation in resonant ultrasonic spectroscopy technique for piezoelectric material [J]. Acta Physica Sinica, 2017, 66(2): 334-341 (in Chinese).
[13] PUJOL J. The solution of nonlinear inverse problems and the Levenberg-Marquardt method [J]. Geophysics, 2007, 72(4): 1-16.
[14] TANG L, ZHANG Y, CAO W. Characterizing full matrix constants of piezoelectric single crystals with strong anisotropy using two samples [J]. Journal of Applied Physics, 2016, 120(16): 164102.
[15] XIANG Y, CHEN C, TANG L, et al. Dielectric, elastic and piezoelectric properties of single domain Pb(Zn1/3Nb2/3)O3-6.5%PbTiO3 single crystal with 3m symmetry measured using one sample [J]. Scripta Materialia, 2021, 194: 113634.
[16] HOLLAND R, EERNISSE E P. Variational evaluation of admittances of multielectroded three-dimensional piezoelectric structures [J]. IEEE Transactions on Sonics and Ultrasonics, 1968, 15(2): 119-131.
[17] OHNO I. Rectangular parallellepiped resonance method for piezoelectric crystals and elastic constants of alpha-quartz [J]. Physics and Chemistry of Minerals, 1990, 17(5): 371-378.
[18] WU X S, CHEN W, LU Y, et al. Vibration analysis of a piezoelectric micromachined modal gyroscope (PMMG) [J]. Journal of Micromechanics and Microengineering, 2009, 19(12): 125008.
[19] MOCHIZUKI E. Application of group theory to free oscillations of an anisotropic rectangular parallelepiped [J]. Journal of Physics of the Earth, 1987, 35: 159-170.
[20] LI H, MA Y, ZHOU Z, et al. Characterizing elastic and piezoelectric constants of piezoelectric materials from one sample using resonant ultrasound spectroscopy [J]. Journal of Materials Science, 2019, 54(9): 6786-6798.
[21] CHEN C, LIU S, TAN X, et al. Accurate characterization of complete set constants of single domain 0.72Pb(Mg1/3Nb2/3)O3-0.28PbTiO3 single crystal by resonant ultrasound spectroscopy using only one sample [J]. Journal of Applied Physics, 2019, 125(6): 064102.
[22] ZHANG Y, TANG L, TIAN H, et al. Determination of temperature dependence of full matrix material constants of PZT-8 piezoceramics using only one sample [J]. Journal of Alloys and Compounds, 2017, 714: 20- 25.

Options
Outlines

/

〈 〉