Effect of Silicon State on Microstructure and Properties of Al-1%Si Alloy During Severe Plastic Deformation

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  • School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240, China

Received date: 2019-12-31

  Online published: 2021-04-02

Abstract

Alloy elements can influence the microstructure evolution of aluminum alloys in the state of solid solute atoms or nano-precipitated silicon particles, but it is still a controversial subject which form has a more significant effect on the microstructure of aluminum alloys. Therefore, taking the Al-1%Si alloy as the research object, the ratio of precipitation state and the solid solution state of the silicon atoms was changed before deformation and a multi-pass accumulative roll-bonding method was used to achieve large deformation. In order to compare the influence of solid solute atoms and nano-precipitated silicon particles on the structure and properties of aluminum alloy during deformation, a comparative study was conducted on the evolution of nano-precipitated silicon particles, grain size, and dislocation density in the process of reaching the saturation state of the microstructure and mechanical properties. The results show that the initial samples with less nano-precipitated silicon particles and more solute silicon atoms have a higher saturated dislocation density and a smaller saturated grain size after deformation, corresponding to a higher saturated yield strength. Solid solute silicon atoms dispersed in the Al-1%Si alloy have a better overall effect than nano-precipitated silicon particles of the same volume in preventing the dynamic recovery of dislocations, which is consistent with the theoretical analysis of dislocations. The dislocation recovery ability in the material affects its saturated grain size. The stronger the dislocation recovery capacity, the larger the saturated grain size.

Cite this article

TANG Jingzhao, YAN Jiawei, SHEN Yao . Effect of Silicon State on Microstructure and Properties of Al-1%Si Alloy During Severe Plastic Deformation[J]. Journal of Shanghai Jiaotong University, 2021 , 55(3) : 249 -257 . DOI: 10.16183/j.cnki.jsjtu.2020.001

References

[1] WANG H , GENG H W , ZHOU D S , et al . Multiple strengthening mechanisms in high strength ultrafine-grained Al-Mg alloys[J]. Materials Science and Engineering: A , 2020, 771: 138613.
[2] CUBERO-SESIN J M , ARITA M , WATANABE M , et al . High strength and high electrical conductivity of UFG Al-2Fe alloy achieved by high-pressure torsion and aging[J]. IOP Conference Series: Materials Science and Engineering , 2014, 63: 012117.
[3] BACHMAIER A , HAFOK M , PIPPAN R . Rate independent and rate dependent structural evolution during severe plastic deformation[J]. Materials Transactions , 2010, 51(1): 8-13.
[4] SUN L , ZHANG Q C , YAN S P , et al . Effect of solute atoms and precipitated phase in Al-4.5wt% Cu alloys on the spatiotempopal characteristics of the serrated yielding[J]. Acta Physica Sinica (Chinese Edition), 2007, 56(6): 3411-3417.
[5] ATODIRESEI M , GREMAUD G , SCHALLER R . Study of solute atom-dislocation interactions in Al-Mg alloys by mechanical spectroscopy[J]. Materials Science and Engineering: A , 2006, 442(1/2): 160-164.
[6] EDALATI K , AKAMA D , NISHIO A , et al . Influence of dislocation-solute atom interactions and stacking fault energy on grain size of single-phase alloys after severe plastic deformation using high-pressure torsion[J]. Acta Materialia , 2014, 69: 68-77.
[7] HUANG T L , WU G L , HUANG X , et al . Characterization of Si particles and their effects on and recrystallization in a nanostructured cold rolled Al-1%Si alloy[J]. IOP Conference Series: Materials Science and Engineering , 2015, 89: 012028.
[8] CHEN Y L , HUANG T L , GONG X , et al . Formation of a random recrystallization texture in heavily cold rolled and annealed Al-1%Si alloy[J]. Materials Science Forum , 2013, 753: 243-246.
[9] 黄天林 . 纳米结构Al-1%Si合金的组织、热稳定性及力学行为研究[D]. 重庆: 重庆大学,2014.
[9] HUANG Tianlin . Structure, thermal stability and mechanical behavior of nanostructured Al-1%Si alloy[D]. Chongqing: Chongqing University, 2014.
[10] HUANG T L , DONG Q S , GONG X , et al . Cold rolled nanostructured super-pure Al (99.9996%) containing 1% Si particles: Structure and strength[J]. Journal of Materials Science , 2012, 47(22): 7914-7920.
[11] OZAWA E , KIMURA H . Excess vacancies and the nucleation of precipitates in aluminum-silicon alloys[J]. Acta Metallurgica , 1970, 18(9): 995-1004.
[12] LASAGNI F , MINGLER B , DUMONT M , et al . Precipitation kinetics of Si in aluminium alloys[J]. Materials Science and Engineering: A , 2008, 480(1/2): 383-391.
[13] GARCíA-INFANTA J M , SWAMINATHAN S , CEPEDA-JIMéNEZ C M , et al . Enhanced grain refinement due to deformation-induced precipitation during ambient-temperature severe plastic deformation of an Al-7%Si alloy[J]. Journal of Alloys and Compounds , 2009, 478(1/2): 139-143.
[14] GUTIERREZ-URRUTIA I , MU?OZ-MORRIS M A , MORRIS D G . Contribution of microstructural parameters to strengthening in an ultrafine-grained Al-7% Si alloy processed by severe deformation[J]. Acta Materialia , 2007, 55(4): 1319-1330.
[15] MU?OZ MORRIS M A , GUTIERREZ-URRUTIA I , MORRIS D G . The effect of geometrically necessary dislocations on grain refinement during severe plastic deformation and subsequent annealing of Al-7%Si[J]. Materials Science and Engineering: A , 2008, 493(1/2): 141-147.
[16] LIU M W , FU H , TIAN L X , et al . Nucleation and growth mechanisms of nano-scaled Si precipitates in Al-7Si supersaturated solid solution[J]. Materials & Design , 2017, 121: 373-382.
[17] NAKAGAWA K , KANADANI T , HASHIMOTO H . Microstructural changes at the initial stage of precipitation in Al-1.2%Si alloys[J]. Journal of the Japan Institute of Metals and Materials , 2003, 67(10): 521-527.
[18] GUTIERREZ-URRUTIA I , MU?OZ-MORRIS M A , MORRIS D G . The effect of coarse second-phase particles and fine precipitates on microstructure refinement and mechanical properties of severely deformed Al alloy[J]. Materials Science and Engineering: A , 2005, 394(1/2): 399-410.
[19] PANIGRAHI S K , JAYAGANTHAN R . Influence of solutes and second phase particles on work hardening behavior of Al 6063 alloy processed by cryorolling[J]. Materials Science and Engineering: A , 2011, 528(7/8): 3147-3160.
[20] TSUJI N , SAITO Y , LEE S H , et al . ARB (accumulative roll-bonding) and other new techniques to produce bulk ultrafine grained materials[J]. Advanced Engineering Materials , 2003, 5(5): 338-344.
[21] TSUJI N , ITO Y , SAITO Y , et al . Strength and ductility of ultrafine grained aluminum and iron produced by ARB and annealing[J]. Scripta Materialia , 2002, 47(12): 893-899.
[22] HUANG T L , SHUAI L F , WAKEEL A , et al . Strengthening mechanisms and Hall-Petch stress of ultrafine grained Al-0.3%Cu[J]. Acta Materialia , 2018, 156: 369-378.
[23] PARK K T , KWON H J , KIM W J , et al . Microstructural characteristics and thermal stability of ultrafine grained 6061 Al alloy fabricated by accumulative roll bonding process[J]. Materials Science and Engineering: A , 2001, 316(1/2): 145-152.
[24] FLEISCHER R L . Rapid solution hardening, dislocation mobility, and the flow stress of crystals[J]. Journal of Applied Physics , 1962, 33(12): 3504-3508.
[25] ZHANG Z , CHEN D L . Consideration of Orowan strengthening effect in particulate-reinforced metal matrix nanocomposites: A model for predicting their yield strength[J]. Scripta Materialia , 2006, 54(7): 1321-1326.
[26] LIU M W , ZHENG R X , XIAO W L , et al . Concurrent enhancement of strength and ductility for Al-Si binary alloy by refining Si phase to nanoscale[J]. Materials Science and Engineering: A , 2019, 751: 303-310.
[27] SONG T , XU X J , FAN Z , et al . Effects of enhanced solid solution treatment on microstructure and dislocation strengthening of Sr microalloyed 2099 type Al-Li alloy[J]. Rare Metal Materials and Engineering , 2012, 41: 373-376.
[28] HUANG F , TAO N R , LU K . Effects of impurity on microstructure and hardness in pure Al subjected to dynamic plastic deformation at cryogenic temperature[J]. Journal of Materials Science & Technology , 2011, 27(7): 628-632.
[29] VALIEV R Z , LANGDON T G . Principles of equal-channel angular pressing as a processing tool for grain refinement[J]. Progress in Materials Science , 2006, 51(7): 881-981.
[30] YAN F , ZHANG H W , TAO N R , et al . Quantifying the microstructures of pure Cu subjected to dynamic plastic deformation at cryogenic temperature[J]. Journal of Materials Science & Technology , 2011, 27(8): 673-679.
[31] MALEKJANI S , HODGSON P D , CIZEK P , et al . Strain rate effect on the cyclic deformation response of UFG Al alloys[J]. Materials Science and Engineering: A , 2012, 548: 69-74.
[32] LI X Y , WEI Y J , YANG W , et al . Competing grain-boundary- and dislocation-mediated mechanisms in plastic strain recovery in nanocrystalline aluminum[J]. Proceedings of the National Academy of Sciences of the United States of America , 2009, 106(38): 16108-16113.
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